Nuclear magnetic resonance spectroscopy of proteins (usually abbreviated protein NMR) or preparation of the sample in a stretched polyacrylamide gel. 12 Sample Preparation and Insertion, Locking and Shimming Sample Preparation Unless you are doing solids NMR, you will need to dissolve your sample in a solvent. 1234 Hach Hall 515-294-5805 www.cif.iastate.edu NMR Sample Preparation 03/19/2013 S.D.C Location: 1232 Hach Hall Contact: Shu Xu or Sarah Cady, 1234 Hach Hall How to Obtain a Quality NMR Spectrum; 1 Properly prepare your sample -- Make sure your sample is "clean" 2 Make sure your tube is clean, i.e. avoid NMR Sample Preparation. The quality of your spectrum is greatly affected by the sample preparation. The NMR Facility does not supply NMR tubes or deuterated solvents.
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